5-Bromo-2-(4-fluoro­phen­yl)-3-phenyl­sulfinyl-1-benzofuran

نویسندگان

  • Pil Ja Seo
  • Hong Dae Choi
  • Byeng Wha Son
  • Uk Lee
چکیده

In the title compound, C(20)H(12)BrFO(2)S, the 4-fluoro-phenyl ring makes a dihedral angle of 2.63 (6)° with the mean plane of the benzofuran fragment. The dihedral angle between the phenyl ring and the mean plane of the benzofuran fragment is 84.60 (6)°. In the crystal, mol-ecules are linked by weak inter-molecular C-H⋯O hydrogen bonds, and slipped π-π inter-actions between the benzene rings of neighbouring mol-ecules [centroid-centroid distance = 3.719 (3) Å, inter-planar distance = 3.000 (3) Å and slippage = 1.520 (3) Å].

منابع مشابه

5-Chloro-2-(4-fluoro­phen­yl)-3-phenyl­sulfinyl-1-benzofuran

In the title compound, C(20)H(12)ClFO(2)S, the O atom and the phenyl ring of the phenyl-sulfinyl substituent lie on opposite sides of the plane of the benzofuran fragment; the phenyl ring is almost perpendicular to this plane [82.44 (5)°]. The 4-fluoro-phenyl ring is rotated out of the benzofuran plane, making a dihedral angle of 20.83 (6)°.

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2-(4-Fluoro­phen­yl)-5,6-methyl­enedi­oxy-3-phenyl­sulfinyl-1-benzofuran monohydrate

In the title compound, C(21)H(13)FO(4)S·H(2)O, the dihedral angles between the mean plane of the benzofuran fragment (r.m.s. deviation = 0.005 Å) and the pendant 4-fluoro-phenyl and phenyl rings are 6.24 (7) and 83.39 (6)°, respectively. In the crystal, mol-ecules are linked by O-H⋯O and C-H⋯O hydrogen bonds.

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2-(4-Fluoro­phen­yl)-5-iodo-3-phenyl­sulfinyl-1-benzofuran

In the title compound, C(20)H(12)FIO(2)S, the dihedral angles between the mean plane [r.m.s. deviation = 0.014 (1) Å] of the benzofuran fragment and the pendant 4-fluoro-phenyl and phenyl rings are 8.0 (1) and 86.06 (6)°, respectively. In the crystal, mol-ecules are linked by weak C-H⋯O hydrogen bonds. The crystal structure also exhibits weak π-π inter-actions between the furan and benzene ring...

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5-Bromo-2-phenyl-3-phenyl­sulfinyl-1-benzofuran

In the title compound, C(20)H(13)BrO(2)S, the O atom and the phenyl group of the phenyl-sulfinyl substituent are located on opposite sides of the plane of the benzofuran system. The S-bound phenyl ring is almost perpendicular to this plane [80.35 (8)°]. The phenyl ring in the 2-position is twisted with respect to the benzofuran plane, making a dihedral angle of 16.0 (1)°.

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2-(4-Bromo­phen­yl)-5-fluoro-3-phenyl­sulfinyl-1-benzofuran

In the title compound, C(20)H(12)BrFO(2)S, the O atom and the phenyl group of the phenyl-sulfinyl substituent lie on opposite sides of the plane through the benzofuran fragment; the phenyl ring is nearly perpendicular to this plane [dihedral angle = 86.98 (6)°]. The 4-bromo-phenyl ring is rotated slightly out of the benzofuran plane, making a dihedral angle of 1.56 (8)°. The crystal structure f...

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عنوان ژورنال:

دوره 67  شماره 

صفحات  -

تاریخ انتشار 2011